ࡱ> fe I@\p Rick Greene Ba= =hKL,8G@"1Arial1Arial1Arial1Arial1Arial1Arial1Arial1Arial1Arial"$"#,##0_);\("$"#,##0\)!"$"#,##0_);[Red]\("$"#,##0\)""$"#,##0.00_);\("$"#,##0.00\)'""$"#,##0.00_);[Red]\("$"#,##0.00\)7*2_("$"* #,##0_);_("$"* \(#,##0\);_("$"* "-"_);_(@_).))_(* #,##0_);_(* \(#,##0\);_(* "-"_);_(@_)?,:_("$"* #,##0.00_);_("$"* \(#,##0.00\);_("$"* "-"??_);_(@_)6+1_(* #,##0.00_);_(* \(#,##0.00\);_(* "-"??_);_(@_)0.0 mm/dd/yy 0.000                + ) , *       @ @ ! ! " " ! !  !  !X     !X !   h !  H   H `4Sample Description[BMetals GPCBs$yDioxins,Furans,Coplanar PCBsY OC PesticidesMethods and QA`i IBDelaware Department of Natural Resources and Environmental Control 2. DNREC Laboratory Data Files.Metals Results PCB Results$Concentrations are in ng/g (ppb) wet,A. PCB Congener Data, ng/g wet weight basis!Concentrations in pg/g (pptr) wetGA. Dioxin/Furan Raw Data, pg/g wet weight basis, analyzed by HRGC/HRMS Organochlorine Pesticide Results Concentrations in ng/g (ppb) wet(cm)(gm)Fillet Skin OnDelaware EstuaryMouth of Delaware Bay Striped BassMeanMinimumMaximumDatePortionLengthWeight Sample ID WaterbodyLocationLatitude LongitudeSampledSpeciesAnalyzed in Sample No.of FishNotes: Delaware Bay% Lipid8 DiU( 1.23)U( .614)U( .616)18 TriU( 1.12)28 TriU( .635)37 Tri42 Tetra44 TetraU( 1.38)47 Tetra49 Tetra52 Tetra60 Tetra64 Tetra66 Tetra70 Tetra74 Tetra80 Tetra82 PentaU( 3.16)87 Penta91 Penta92 PentaU( .617)95 PentaU( 2.79)U( 2.34)99 Penta 105 Penta 110 Penta 114 PentaU( 2.62)U( 2.81)118Penta 119 Penta 120 PentaU( 1.67)U( 1.3) 123 Penta137 Hexa141 Hexa146 Hexa149 Hexa151 Hexa153 Hexa156 Hexa157 Hexa166 Hexa168 Hexa 170,190 Hepta171HeptaU( 1.15) 174 HeptaU( 1.22) 177 HeptaU( 1.18) 179 Hepta 180 Hepta 183 Hepta 185 Hepta 187 Hepta 189 Hepta 191 Hepta194 OctaU( 1.54)195 OctaU( 1.9) 196,203OctaU( 1.69)198 OctaU( 2.92)U( 1.89)200 OctaU( 1.61)201 OctaU( 1.35)U( 2.35)205 Octa206Nona207 Nona208 Nona209 DecaSum of Congeners U( 2.67 empc) U( 1.36 empc) U( 2.1 empc) U( 1.35 empc) U( 2.71 empc) U( 1.15 empc) U( 1.18 empc) U( 2.62 empc) U( 2.93 empc) U( 3.58 empc) U( 3.33 empc) U( 4.31 empc) U( 1.24 empc) U( 1.5 empc) U( 1.14 empc) U( .72 empc) U( .841 empc) U( 2.44 empc) U( 1.86 empc) U( 1.32 empc) U( 1.28 empc) U( .94 empc) U( 1.75 empc) U( 1.31 empc) U( 10.2 empc) U( 1.66 empc) U( 3.53 empc) U( 1.46 empc) U( 1.45 empc)Y1. U(#)=Compound not detected. Value in parentheses is the instrumental detection limit.+B. PCB Homolog Data, ng/g wet weight basisMonoDiTriTetraPentaHexaHeptaOctaNonaDecaSum of HomologsOCDFOCDDU( 2.38)U( 4.78)U( 4.98)U( 3.94)U( 3.98)Sum of DDD, DDE, DDT cis-Chlordanetrans-ChlordaneU( 10.4)cis -Nonachlortrans- NonachlorU( 5.12) OxychlordaneSum of Chlordanes:DicofolDieldrin Endosulfan I Endosulfan IIEndrinHeptaclor epoxideHexachlorobenzeneU( 2.55)LindaneMirex A. MethodsiSamples were collected by the Delaware Department of Natural Resources and Environmental Control (DNREC).iOrganic contaminants were analyzed by the Midwest Research Institute (MRI) under contract with the DNREC.Field procedures for sample collection followed DNREC ESS Standard Operating Procedure No. 500 ("Field Procedures for Fish Sample Handling").Procedures for dissection, tissue grinding, and sample storage followed DNREC ESS Standard Operating Procedure No. 501 ("Processing of Finfish for Chemical Analyis"). CLaboratory methods for organic contaminants are fully described in:)Briefly with regard to chemical analyses,Dioxins, furans, and coplanar PCB congeners were analyzed by High Resolution Gas Chromatography/High Resolution Mass Spectrometry (HRGC/HRMS).}All other organic compounds were analyzed by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS).B. Quality AssuranceQuality assurance procedures for organic analyses included method blanks, matrix spikes, matrix spike duplicates, and percent recoveries for internal standardsBand surrogate standards. Results of QA testing are documented in: U( 3.95 empc) U( 12.6 empc) U( 28 empc)QB. Non-Ortho Coplanar PCB Raw Data, pg/g wet weight basis, analyzed by HRGC/HRMSRData and information in this spreadsheet were obtained from the following sources: Total TCDF Total TCDD Total PECDF Total PECDD Total HXCDF Total HXCDD Total HPCDF Total HPCDD 2,3,7,8-TCDD1,2,3,7,8-PeCDF2,3,4,7,8-PeCDF1,2,3,7,8-PeCDD1,2,3,4,7,8-HxCDF1,2,3,6,7,8-HxCDF2,3,4,6,7,8-HxCDF1,2,3,7,8,9-HxCDF1,2,3,4,7,8-HxCDD1,2,3,6,7,8-HxCDD1,2,3,7,8,9-HxCDD1,2,3,4,6,7,8-HpCDF1,2,3,4,7,8,9-HpCDF1,2,3,4,6,7,8-HpCDD 2,3,7,8-TCDF2. U(# empc)=Compound not detected. Value in parentheses is the estimated maximum possible concentration (empc) detection limit based on an interference.Sample Descriptiono,p'-DDDp,p'-DDDo,p'-DDEp,p'-DDEo,p'-DDTp,p'-DDT0Dioxin, Furan, and Coplanar PCB Congener Results 38 50 36.0 75 03 18.1M1994 Study of Contaminants in Striped Bass from the Mouth of the Delaware Bay1. Midwest Reseach Institute. 1996. Analysis of Fish Tissue Samples for PCDDs, PCDFs, Congener-Specific PCBs, and Pesticides Final Report (MRI Project No. 4072-01). Report prepared by the Midwest Research Institute for the Delaware Department of = Natural Resources and Environmental Control, Dover, DE.1Metals were not analyzed as a part of this study.Lipid % 1 Mono3 MonoU( .306)U( .19)U( .627)4 DiU( .222)U( .552)U( .378)U( .291)U( .597)7 DiU( .159)U( .308)U( .162)U( .141)U( .11)U( .273)U( .187)U( .144)U( .295)U( .359)U( .582)U( .372)U( .242)U( .202)U( .271)U( .251)U( .293)U( .296)U( 2.77)U( 3.48)U( 4.22)84 Penta86 PentaU( 2.88)U( 3.41)U( 1.62)U( 3.58)U( 1.85)U( 3.39)U( 4.11)97 PentaU( 3.49)U(3.57) 101 PentaU(5.01)U( 1.88)U( 2.37)U( 2.87)U( 2.11)U( 3.02)128 HexaU( .292)U( .246)U( .409)U( .394)U( .5) 138,158 HexaU( .618)U( .596)U( .396)U( .756)U( .425)U( .27)U(.285)U( .204)167 HexaU( .681)U( .761)U( .383)U( .662)U( .762)U( .429)U( .452)U( .504)U( 1.59)U( 3.78)U( 4.59)U( 4.1)U( 2.33)U( 5.56)U( 1.92)U( 2.83)U( 3.27)U( .475)U( 1.13)U( .698)U( .808)U( 2.68)U( 3.25)U( 2.9)U( 1.91)U( 9.62)U( 11.2)U( 6.08)U( 5.89)U( 3.17)U( 12.1)U( 11.3)U( 15.9)U( 18.5) Mouth of Bay U( 11.1 empc) U( 13.3 empc) U( 14.5 empc) U( 8.65 empc) U( 7.39 empc) U( .205 empc) U( .571 empc) U( 1.43 empc) U( 4.03 empc) U( 2.59 empc) U( 4.68 empc) U( .334 empc) U( .569 empc) U( .497 empc) U( 2.21 empc) U( 5.42 empc) U( .398 empc) U( .52 empc) U( .543 empc) U( .619 empc) U( .592 empc) U( .911 empc) U( .97 empc) U( 1.19 empc) U( .328 empc) U( .762 empc) U( .754 empc) U( 2.89 empc) U( 4.98 empc) U( .369 empc) U( .388 empc) U( 2.35 empc) U( .43 empc) U( 1.01 empc) U( .439 empc) U( 4.29 empc) U( .228 empc) U( .664 empc) U( .243 empc) U( .587 empc) U( .371 empc) U( .913 empc) U( 1.73 empc) U( .448 empc) U( 1.96 empc) U( 7.61 empc) U( 9.52 empc) U( 6.06 empc) U( 8.99 empc) U( 5.12 empc) U( 7.48 empc) U( 6.19 empc) U( 4.82 empc) U( 7.17 empc) U( 4.85 empc) U( 10.5 empc) U( 6 empc) U( 9.76 empc) U( 4.86 empc) U( 2.32 empc) U( 6.79 empc) U( 5.09 empc) U( 3.65 empc) U( 8.4 empc) U( 13.7 empc) U( 13.1 empc) U( .38 empc) U( .422 empc) U(0.205 empc) U( .423 empc) U(0.732 empc) U( .321 empc) U( 1.42 empc) U( .699 empc) U( .349 empc) U( .554 empc) U( .405 empc) U( .563 empc) U( 1.04 empc) U( .735 empc) U( .613 empc) U( .985 empc) U( 1.4 empc) U( 1.63 empc) U( 3.79 empc) U( 2.95 empc) U( 1.6 empc) U( 2.24 empc) U( 1.3 empc) U( .732 empc) U( 1.07 empc) U( 3.02 empc) U(1.24 empc) U( 1.02 empc) U( 1.11 empc) U( 14.7 empc) U( 15.5 empc) U( 4.15 empc) U( 11.6 empc) U( 6.69 empc) U( 15.9 empc) U( 7.96 empc) U( 9.33 empc) U( 11.4 empc) U( 22.4 empc) U( 11.7 empc) U( .598 empc) U( .999 empc) U(0.733 empc) U( .7 empc) U(2.5 cdl)U(2.5 cdl) (3) 1. U(# empc) = Com< pound not detected. Value in parentheses is an estimated maximum concentration (empc) detection limit based on an interference.^2. U(#)= Compound not detected. Value in parentheses is an instrumental noise detection limit.3. U(# cdl) = Compound not detected. Value in parentheses is a calculated detection limit (cdl) based on the lowest calibration standard.U( .612)U( .609)U( 7.7)U( 3.61)U( 13.5)U( 9.46)U( 4.43)U( 16.6)U( 5.64) U( 8.42 empc) U( .758 empc) U( 3.75 empc) U( 7.04 empc) U( 11.3 empc) U( .737 empc) U( 5.21 empc) U( 2.17 empc) U( 2.72 empc) U( 1.25 empc) U( 14.3 empc) U( 6.18 empc) U( 5.28 empc)U( 8.49)U( 14.9)81-TPCB77-TPCB 127-PePCBU( .49)U( .491)U( .493)U( .487) 126-PePCB 169-HxPCBX1. U(#)=Compound not detected. Value in parentheses is the curve based detection limit.|Midwest Reseach Institute. 1996. Analysis of Fish Tissue Samples for PCDDs, PCDFs, Congener-Specific PCBs, and Pesticides zFinal Report (MRI Project No. 4072-01). Report prepared by the Midwest Research Institute for the Delaware Department of 7Natural Resources and Environmental Control, Dover, DE. U( .494) (1)  U( .617) (1) U( 3.27 empc) (2)U( 2.76)U( .815)U( .462)U( 2.44)U( 1.65)U( 1.11)U(1.8)U( 1.39)U(1.93)UU( 4.73)U( 5.18)U(1040)U(1450)U(110)U( 8.82)U(2010)U(1950)U( .892)U( 1.5)U( 1.53)U( 2)U( 1.48)U( 1.07)U( 6.04)U( 6.61)U( 10.2)U( 11.7)U( 4.37) U(1.08 empc) U(1.92empc) U( 3.72 empc) U( 8.66 empc) U( 4.77 empc) U( 5.95 empc) U( 24.9 empc) U( 713 empc) U( 1250 empc) U( 721 empc) U( 26.3 empc) U( 26.6 empc) U( 10.7 empc) U( 5.9 empc) U(12.5empc) U( 3.64 empc) U( 1.58 empc) U( 1.51 empc) U( .531 empc) U( 3.09 empc) U( 5.74 empc) U( 2.88 empc) U( 3.15 empc) U( 3.21 empc) U( 5.08 empc)U( 2.71)U( 3.15)U( 3)U( 2.07)U( 3.2)U( 1.43)U( 4.65)U( 5.39)U( 1.63)U( 5.15) U( 2.79 empc) U( 3.07 empc) U( 5.76 empc) U( 11.5 empc) U( .99 empc) U( 7.46 empc) U( 1.55 empc) U( 5.06 empc) U( 7.68 empc) U( 2.8 empc) U( 1.59 empc)3. U(# cdl) = Compound not detected. Value in parentheses is calculated detection limit (cdl) based on the lowest calibration standard. 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