ࡱ>  I@\p Clarke Rupert Ba= =hKL,8G@"1Arial1Arial1Arial1Arial1Arial1Arial1Arial1Arial1Arial"$"#,##0_);\("$"#,##0\)!"$"#,##0_);[Red]\("$"#,##0\)""$"#,##0.00_);\("$"#,##0.00\)'""$"#,##0.00_);[Red]\("$"#,##0.00\)7*2_("$"* #,##0_);_("$"* \(#,##0\);_("$"* "-"_);_(@_).))_(* #,##0_);_(* \(#,##0\);_(* "-"_);_(@_)?,:_("$"* #,##0.00_);_("$"* \(#,##0.00\);_("$"* "-"??_);_(@_)6+1_(* #,##0.00_);_(* \(#,##0.00\);_(* "-"??_);_(@_)0.0 mm/dd/yy 0.000                + ) , *       @ @ ! ! " " ! !  !  !X     !X !   h  @ !  H   H ! !P "T@ @ "T `HPSample DescriptionfMetals ~PCBs$Dioxins,Furans,Coplanar PCBs  OC Pesticides=.Methods and QA`i ZBDelaware Department of Natural Resources and Environmental Control 2. DNREC Laboratory Data Files.Metals Results&Concentrations are in units of ppm wet PCB Results$Concentrations are in ng/g (ppb) wet,A. PCB Congener Data, ng/g wet weight basis!Concentrations in pg/g (pptr) wetGA. Dioxin/Furan Raw Data, pg/g wet weight basis, analyzed by HRGC/HRMS Organochlorine Pesticide Results Concentrations in ng/g (ppb) wet(cm)(gm)Red ClayAshland White SuckerFillet Skin On American EelFillet Skin OffStantonRedbreast Sunfish Saint JonesRoute 13 39 08 56.0Channel Catfish White PerchLargemouth BassBarkers White Catfish Silver Lake 39 10 20.0 C & D Canal Lums Pond 39 33 19.0Delaware EstuaryPea Patch Island Collins Beach 39 23 14.7 Leipsic RiverGarrison's Lake Naamans Creek Naamans Road 39 48 47.0Shellpot Creek Smyrna River Lake ComoMeanMinimumMaximumDatePortionLengthWeight Sample ID WaterbodyLocationLatitude LongitudeSampledSpeciesAnalyzed in Sample No.of FishArsenic Cadmium Copper Lead MercurySeleniumZinc (ppm)<0.2<0.02<0.12< 0.2< 0.02<0.201.165.64Notes: Red Clay C&D CanalDelaware River Delaware Bay Lgmouth bass% Lipid Americal Eel8 DiU( 1.23)U( .614)U( .616)U( .803)U( 1.24)U( .622)U( 1.25)U( .615)U( .621)U( .804)U( .624)18 TriU( 1.36)U( 1.16)U( 1.12)U( .901)U( 1.32)U( .62)U( 1.09)U( 1.1)28 TriU( .767)U( .635)37 Tri42 TetraU( .825)U( 1.28)U( 1.33)U( .967)44 TetraU( 1.38)U( .835)U( 1.29)U( .978)47 TetraU( 1.07)U( .648)49 TetraU( 1.27)U( .77)U( 1.19)U( .902)52 TetraU( .753)60 TetraU( .782)64 TetraU( .85)66 TetraU(1.24)U(1.23)U( .86)U( .839)U(.624)70 TetraU( .873)U( .816)74 TetraU( .916)80 TetraU( .752)82 PentaU( 4.13)U( 4.41)U( 3.12)U( 2.56)U( 3.26)U( 1.63)U(2.54)U( 1.01)U(.979)U(.889)U( 3.5) 84/101 PentaU( 3.16)87 Penta91 PentaU( 3.34)U( 1.81)U( 2.25)U( 2.52)U( 2.07)U( 2.64)U( 1.96)U(.614)U(.77)U(.784)U( .685)U( 2.93)92 PentaU( 3.42)U( 1.86)U( 2.31)U( 2.58)U( 2.12)U( 2.01)U( .617)U( .848)U( .799)U( .824)U( .80)U( 3)95 PentaU( 2.79)U( 2.17)U( .777) 97/86 PentaU( 2.34)U( 3.71)U( 2.74)U( 1.47)U( 4.0)U( 2.94)U( 3.05)99 Penta 105 PentaU( 1.79)U( 1.87) 110 Penta 114 PentaU( 3.32)U( 3.55)U( 2.51)U( 2.06)U( 2.62)U(1.26)U(.621)U( .76)U( .737)U( 1.49)U( 2.81)118Penta 119 PentaU( 2.44)U( 1.65)U( 1.84)U( 1.51)U( 1.43)U(.688)U(.62) 120 PentaU( 2.21)U( .779)U( 1.67)U( 1.37)U( 1.75)U( 1.3)U( .735)U( 1.94) 123 PentaU( .668)U( 2.95)U( .966)U( 1.7)U( 1.03)U( .64)U( 2.41)137 HexaU( .934)138 Hexa141 Hexa146 Hexa149 Hexa151 Hexa153 Hexa156 Hexa157 Hexa158 HexaU( .689)166 HexaU( .656) 167/128 Hexa168 Hexa 170,190 HeptaU( .912)171HeptaU( 1.15) 174 HeptaU( 1.22) 177 HeptaU( 1.18) 179 HeptaU( .798) 180 Hepta 183 HeptaU( 1.02) 185 Hepta 187 Hepta 189 Hepta 191 Hepta194 OctaU( 3.92)U( 1.54)U( 1.26)U( 2.19)U( 2.97)U( .938)U( 1.52)195 OctaU( 3.4)U( 2.84)U( 2.23)U( 1.9)U( 2.57)U( 1.66)U( 1.6)U( 3.29)U( .812)U( 6.29)U(2.06) 196,203OctaU( 3.46)U( 2.89)U( 2.26)U( 1.93)U( 1.69)U( .826)U( 6.4)198 OctaU( 1.41)U( 3.86)U( 3.22)U( 2.53)U( 2.15)U( 2.92)U( 1.89)U( 3.73)U( .922)U( 1.5)200 OctaU( 1.61)U( 5.34)201 OctaU( 4.21)U( 1.35)U( 2.76)U( 2.35)U( 4.07)U(1.25)205 OctaU( 2.85)U( .704)206Nona207 Nona208 NonaU( .774)U( .679)209 DecaSum of Congeners U( 2.08 empc) U( 2.22 empc) U( 3.35 empc) U( 1.55 empc) U( .903 empc) U( 2.04 empc) U( 3.29 empc) U( .882 empc) U( 2.29 empc) U( 1.41 empc) U( 1.61 empc) U( 2.67 empc) U( 1.7 empc) U( 1.99 empc) U( 1.62 empc) U( 1.89 empc) U( 2.01 empc) U( 1.03 empc) U( 3.21 empc) U( 1.36 empc) U( 1.06 empc) U( 3.06 empc) U( .997 empc) U( 2.1 empc) U( 2.25 empc) U( 3.57 empc) U( 1.35 empc) U( 1.44 empc) U( 2.68 empc) U( 1.83 empc) U( .809 empc) U( 2.15 empc) U( .744 empc) U( 2.58 empc) U( 2.71 empc) U( 2.34 empc) U( .676 empc) U( 2.13 empc) U( 2.75 empc) U( 2.37 empc) U( .687 empc) U( 2.16 empc) U( 1.8 empc) U( 1.15 empc) U( 1.18 empc) U( 2.62 empc) U( 2.19 empc) U( 2.93 empc) U( 2.66 empc) U( 2.81 empc) U( 4.71 empc) U( 12.9 empc) U( 22.7 empc) U( 3.58 empc) U( 5.82 empc) U( 3.04 empc) U( 4.57 empc) U( 3.44 empc) U( 1.9empc) U(2.51 empc) U( 4.41 empc) U( 5.31 empc) U( 7.18 empc) U( 4.63 empc) U( 3.48 empc) U( 1.78empc) U( 5.11 empc) U( 6.76 empc) U( 4.72 empc) U( 5.17 empc) U( 5.43 empc) U( 5.63 empc) U( 4.48 empc) U( 9.5 empc) U( 3.55 empc) U( 4.4 empc) U( 1.92 empc) U( 1.69 empc) U( 3.33 empc) U(4.46 empc) U( 2.52 empc) U( 3.56 empc) U( 6.65 empc) U( 6.72 empc) U(3.5 empc) U( 2.63 empc) U(3.13 empc) U( 4.24 empc) U( 4.31 empc) U( 4.22 empc) U( 3.61 empc) U( 2.2 empc) U( 4.51 empc) U( 3.63 empc) U( 4.37 empc) U( 4.78 empc) U( 2.94 empc) U( 2.36 empc) U( 5.23 empc) U( 4.91 empc) U( 5.45 empc) U(2.51empc) U( 15 empc) U( 2.91 empc) U( 4.43 empc) U( 3.54 empc) U(4.4empc) U( 3.23 empc) U( 1.84 empc) U( .761 empc) U( 1.27 empc) U( 1.54 empc) U( 1.57 empc) U( 1.24 empc) U( 1.5 empc) U( 1.14 empc) U( 1.21 empc) U( 3.69 empc) U( 5.7 empc) U( 1.98 empc) U( 2.07 empc) U( 1.37 empc) U( .808 empc) U( 1.52 empc) U( 2.48 empc) U( 1.34 empc) U( 1.12 empc) U( .858 empc) U( .72 empc) U( .764 empc) U( .841 empc) U( .725 empc) U( .793 empc) U(0.799 empc) U( .939 empc) U( .695 empc) U( 2.44 empc) U( 1.86 empc) U( 1.81 empc) U( .638 empc) U( .848 empc) U( 1.53 empc) U( 1.32 empc) U( 2.28 empc) U( 2.69 empc) U( .807 empc) U( .831 empc) U( .742 empc) U( .78 empc) U( 1.48 empc) U( 1.28 empc) U( .718 empc) U( 2.38 empc) U( .94 empc) U( 1.16 empc) U( 1.49 empc) U( .86 empc) U(0.72 empc) U( .928 empc) U( .769 empc) U( .642 empc) U( .803 empc) U( 1.75 empc) U( 1.31 empc) U( 1.13 empc) U( .931 empc) U( 3.28 empc) U( 3.66 empc) U( 4.38 empc) U( .775 empc) U( .902 empc) U( 2.83 empc) U( 1.51 empc) U( 3.01 empc) U( 3.94 empc) U( 5.93 empc) U( 8.53 empc) U( 10.2 empc) U( 4.32 empc) U( .785 empc) U( 2 empc) U( 2.02 empc) U( 4.05 empc) U( 8.12 empc) U( 8.03 empc) U( 6.42 empc) U( 2.33 empc) U( 9.09 empc) U( .853 empc) U( 3.62 empc) U( 2.98 empc) U( .859 empc) U( 2.06 empc) U( 1.66 empc) U( 8.48 empc) U( 6.26 empc) U( 4.79 empc) U( 90.6 empc) U( 3.82 empc) U( 3.03 empc) U( 6.81 empc) U( 3.53 empc) U( 1.65 empc) U( 3.46 empc) U( 1.78 empc) U( 2.18 empc) U( 4.39 empc) U( 1.46 empc) U( 4.73 empc) U( .766 empc) U( 1.39 empc) U( 1.45 empc) U( 1.23) (1) U( 4.42 empc) (2)Y1. U(#)=Compound not detected. Value in parentheses is the instrumental detection limit.+B. PCB Homolog Data, ng/g wet weight basisMonoDiTriTetraPentaHexaHeptaOctaNonaDecaRedbreast sunfishSum of HomologsU( 3.06 empc) (2)Channel Catfish U(0.110)U(0.058)U(0.073)U(0.149)OCDFOCDDU(0.25)U(0.454)U( 2.4)U( 4.74)U( 4.77)U( 4.72)U( 2.39)U( 2.36)U( 2.38)U( 6.95)U( 4.78)U( 4.73)U( 2.5)U( 2.48)U( 4.92)U( 2.45)U( 2.46)U( 4.94)U( 4.97)U( 8.74)U( 4.98)U( 2.59)U( 10.6)U(3.22)U( 4.93)U( 2)U( 3.94)U( 3.95)U( 3.76)U( 3.98)U( 1.99)U( 1.97)< U( 8.54)U( 2.49)U( 2.65)U( 8.23)Sum of DDD, DDE, DDT cis-ChlordaneU( 7.47)trans-ChlordaneU( 7.19)U( 10.4)U( 8.01)U( 6.42)U( 4.99)U( 10.3)U( 2.82)U( 25.6)cis -Nonachlortrans- NonachlorU( 5.12)U( 5.13)U( 5.17)U( 5.18) OxychlordaneSum of Chlordanes:DicofolDieldrinU( 12.3)U( 8.76)U( 46.2)U( 9.23)U( 16.2)U( 13.9)U( 20.1)U( 32.3)U( 72.8)U( 47)U( 11.5) Endosulfan IU( 463)U( 21.2)U( 585)U( 47.1)U( 329)U( 12.2)U( 94.5)U( 603)U(43.1)U( 6.37)U( 218)U( 118)U( 84.2)U(2800) Endosulfan IIU( 62.5)U( 130)U( 38.2)U( 25.1)U( 41.7)EndrinU(22.3)U( 6.77)U( 16.9)U( 7.79)U( 41.1)U( 8.21)U( 8.11)U( 14.4)U( 9.99)U( 17.9)U( 28.7)U( 38.4)U( 12.4)U( 64.8)U( 41.8)Heptaclor epoxideHexachlorobenzeneU( 2.55)U( 5.02)U( 5.03)U( 5.07)U( 2.54)U( 5.08)LindaneMirex A. MethodsiSamples were collected by the Delaware Department of Natural Resources and Environmental Control (DNREC).TMetals were analyzed by the DNREC's Environmental Services Section (ESS) Laboratory.iOrganic contaminants were analyzed by the Midwest Research Institute (MRI) under contract with the DNREC.Field procedures for sample collection followed DNREC ESS Standard Operating Procedure No. 500 ("Field Procedures for Fish Sample Handling").Procedures for dissection, tissue grinding, and sample storage followed DNREC ESS Standard Operating Procedure No. 501 ("Processing of Finfish for Chemical Analyis"). WLaboratory methods for metals are described in DNREC ESS Standard Operating Procedures.CLaboratory methods for organic contaminants are fully described in:)Briefly with regard to chemical analyses,Metals other than mercury and zinc were analyzed using Graphite Furnace Atomic Absorption (GFAA). Zinc was analyzed using Inductively Coupled Argon Plasma (ICAP).LMercury was analyzed using Cold Vapor Atomic Absorption Spectrometry (CVAA).Dioxins, furans, and coplanar PCB congeners were analyzed by High Resolution Gas Chromatography/High Resolution Mass Spectrometry (HRGC/HRMS).}All other organic compounds were analyzed by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS).B. Quality AssuranceQuality assurance testing for metals included matrix spike and matrix spike duplicate analyses. Results of those analyses are on file at the DNREC ESS Laboratory.Quality assurance procedures for organic analyses included method blanks, matrix spikes, matrix spike duplicates, and percent recoveries for internal standardsBand surrogate standards. Results of QA testing are documented in: U( 5.97 empc) U( 4.87 empc) U( 6.68 empc) U( 20.1 empc) U( 23.4 empc) U( 20.8 empc) U( 3.95 empc) U( 30.6 empc) U( 10.4 empc) U( 32.1 empc) U( 6.31 empc) U( 6.02 empc) U( 3.9 empc) U( 16.1 empc) U( 20 empc) U( 12.6 empc) U( 11.2 empc) U( 16.8 empc) U( 20.2 empc) U( 21.3 empc) U( 18.4 empc) U( 28 empc) U( 18.5 empc) U( 30.4 empc) U( 101 empc) U( 32.5 empc) U( 26.6 empc) U( 82.4 empc) U( 65 empc) U( 16.6 empc) U( 24.4 empc) U( 6.87 empc) U( 6.99 empc) U( 3.7 empc) U( 6.82 empc) U( 7.62 empc) U( 91.1 empc) U( 2.03 empc) U( 4.92) (1) U( 27.4 empc) (2)U(0.067) U(0.672 empc)U(0.283) U(0.675 empc) U(0.170 empc) U(0.391 empc) U(0.240 empc) U(0.869 empc)U(0.027) U(0.226 empc) U(0.319 empc) U(0.474 empc) U(0.343 empc)U(0.085)U(0.182)U(0.237) U(0.322 empc) U(0.686 empc)U(0.246 empc) U(0.710 empc) U(0.137 empc)U(0.087)U(0.035)U(0.244) U(0.423 empc)U(0.345 empc) U(0.545 empc) U(1.09 empc) U(0.249 empc)U(0.143) U(0.311 empc) U(0.788 empc) U(0.571 empc)U(1.38)U(0.927) U(0.792 empc) U(0.073 empc)U(1.08)U(0.466) U(0.349 empc)U(1.27)U(0.778) U(0.606 empc)U(1.46)U(0.728)U(0.374)U(0.218)U(0.426)U(1.15)U(0.854)U(0.709) U(0.117 empc)U(0.996)U(0.429)U(0.602)U(1.17)U(0.717)U(0.376)U(1.34)U(0.670)U(0.345) U(0.274 empc) U(0.369 empc)U(0.211)U(1.3)UD(1.43)U(0.957)U(0.794) U(0.173 empc)U(1.12)U(0.452)U(0.675)U(1.32)U(0.804)U(0.421)U(1.50)U(0.751)U(0.387)U(0.248)U(0.297)U(0.579)U(1.57)U(1.73)U(1.16)U(0.963)U(0.054)U(1.35)U(0.584)U(0.818)U(1.60)U(0.975)U(0.511)U(1.82)U(0.911)U(0.469)U(0.219) U(0.554 empc)U(0.155)U(0.239)U(0.047)U(0.103)U(0.068) U(0.093 empc) U(0.433 empc) U(0.108 empc)U(0.35)U(0.179)U(0.096)U(0.32) U(0.498 empc)U(0.212)U(0.306)U(0.15)U(0.231)U(1.00) U(0.256 empc) U(0.338 empc) U(0.060 empc) U(0.144 empc)U(0.34)U(0.173) U(0.097 empc) U(0.242 empc)U(1.86)U(0.989)U(.505)U(0.129)U(0.242) U(1.49 empc) U(0.681empc) U(0.383 empc)U(0.256)U(0.280) U(0.536 empc)U(1.94)U(0.618)U(0.53)U(0.414)U(0.351)U(0.904)U(2.35)U(1.11)U(0.637)U(0.163)U(0.305)U(0.448)U(0.494)U(0.266)U(0.323)U(0.354)U(0.587)U(2.45)U(0.780)U(0.66)U(0.522)U(0.443) U(1.30 empc) U(0.621 empc) U(0.223 empc) U(0.148 empc) U(0.0975) U(0.111 empc)U(0.013) U(0.207 empc) U(0.0139)U(0.012) U(0.0274)U(0.042) U(0.0350)U(0.052)U(1.30)U(1.43)U(0.962)U(0.799)U(0.484)U(0.678)U(0.808)U(0.424)U(1.51)U(0.755)U(0.389) U(0.0995)U(0.337)U(2.08)U(0.564)U(0.144)U(0.270)U(0.396)U(0.437)U(0.235)U(0.285)U(0.313)U(0.519)U(2.17)U(0.690)U(0.588)U(0.392)U(0.020)U(.685)QB. Non-Ortho Coplanar PCB Raw Data, pg/g wet weight basis, analyzed by HRGC/HRMSU(1.92)n1. U(#)=Compound not detected. Value in parentheses is the detection limit based on 2.5 X instrumental noise.U(1.43 empc) (2)  U(0.138) (1) U(6.22 empc) (2) RData and information in this spreadsheet were obtained from the following sources: Total TCDF Total TCDD Total PECDF Total PECDD Total HXCDF Total HXCDD Total HPCDF Total HPCDD 2,3,7,8-TCDD1,2,3,7,8-PeCDF2,3,4,7,8-PeCDF1,2,3,7,8-PeCDD1,2,3,4,7,8-HxCDF1,2,3,6,7,8-HxCDF2,3,4,6,7,8-HxCDF1,2,3,7,8,9-HxCDF1,2,3,4,7,8-HxCDD1,2,3,6,7,8-HxCDD1,2,3,7,8,9-HxCDD1,2,3,4,6,7,8-HpCDF1,2,3,4,7,8,9-HpCDF1,2,3,4,6,7,8-HpCDD 2,3,7,8-TCDF77-TCB81-TCB126-PeCB127-PeCB169-HxCB2. U(# empc)=Compound not detected. Value in parentheses is the estimated maximum possible concentration (empc) detection limit based on an interference.1. Midwest Reseach Institute. 1997. Analysis of Fish Tissue Samples for PCDDs, PCDFs, Congener-Specific PCBs, and Pesticides f Institute for the Delaware Department of Natural Resources and Environmental Control, Dover, DE. from Selected Delaware Stream Basins, FY '96 Final Report (MRI Project No. 4485-01). Report prepared by the Midwest Research |Midwest Reseach Institute. 1997. Analysis of Fish Tissue Samples for PCDDs, PCDFs, Congener-Specific PCBs, and Pesticides ~from Selected Delaware Stream Basins, FY '96 Final Report (MRI Project No. 4485-01). Report prepared by the Midwest Research `Institute for the Delaware Department of Natural Resources and Environmental Control, Dover, DE.0.555 J0.596 J0.392 J1.18 J0.844 J0.705 J0.58 J0.815 J0.250 J0.462 J0.304 J0.507 J0.249 J0.871 J0.358 J0.772 J0.859 J0.179 J0.736 J0.101 J2.97 J0.962 J0.36 J0.298 J0.295 J0.115 J0.716 J0.118 J0.3 J0.366 J0.584 J0.774 J1.08 J0.404 J0.762 J0.192 J0.441 J0.188 J0.691 J0.079 J2.045 J0.143 J0.287 J0.979 J0.63 J0.795 J0.176 J0.436 J0.218 J0.178 J0.323 J0.345 J0.087 J0.144 J0.435 J0.529 J0.091 J0.13 J0.226 J0.464 J1.4 J0.217 J0.348 J0.356 J0.127 J0.901 J0.625 J0.62 J1.12 J0.337 J0.156 J<70.798 J1.16 J0.457 J0.266 J2.16 J0.495 J0.312 J0.327 J0.543 J1.55 J0.719 J0.131 J0.219 J0.2 J0.074 J0.899 J0.269 J0.102 J0.493 J0.18 J0.565 J1.48 J0.509 J U(1.06) (1)U(0.643)=3. 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