ࡱ>  I@\p Clarke Rupert Ba= =X\+8;@"1Arial1Arial1Arial1Arial1Arial1Arial1Arial1Arial1Arial"$"#,##0_);\("$"#,##0\)!"$"#,##0_);[Red]\("$"#,##0\)""$"#,##0.00_);\("$"#,##0.00\)'""$"#,##0.00_);[Red]\("$"#,##0.00\)7*2_("$"* #,##0_);_("$"* \(#,##0\);_("$"* "-"_);_(@_).))_(* #,##0_);_(* \(#,##0\);_(* "-"_);_(@_)?,:_("$"* #,##0.00_);_("$"* \(#,##0.00\);_("$"* "-"??_);_(@_)6+1_(* #,##0.00_);_(* \(#,##0.00\);_(* "-"??_);_(@_) mm/dd/yy0.0                + ) , *       H "   " ! ! ! ! !X   H   !X !  h ! !    @ "T !P  D `m5Sample DescriptionKMetals !aPCBs$4Dioxins,Furans,Coplanar PCBs OC Pesticides4"Methods and QA`i ` BDelaware Department of Natural Resources and Environmental ControlRData and information in this spreadsheet were obtained from the following sources:f Institute for the Delaware Department of Natural Resources and Environmental Control, Dover, DE. 2. DNREC Laboratory Data Files.MeanMinimumMaximumDatePortion No.of FishLengthWeight Sample ID WaterbodyLocationLatitude LongitudeSampledSpeciesAnalyzed in Sample(cm)(gm)Delaware Estuary Delaware Bay Striped BassFillet Skin OnCherry Island FlatsRed Clay CreekYorklyn Brown Trout AppoquiniminkNoxontown PondLargemouth Bass1. Midwest Reseach Institute. 1998. Analysis of Fish Tissue Samples for PCDDs, PCDFs, Congener-Specific PCBs, and Pesticides from Selected Delaware Stream Basins, FY '98 Final Report (MRI Project No. 4892). Report prepared by the Midwest Research Metals Results&Concentrations are in units of ppm wet PCB Results$Concentrations are in ng/g (ppb) wet,A. PCB Congener Data, ng/g wet weight basis!Concentrations in pg/g (pptr) wetGA. Dioxin/Furan Raw Data, pg/g wet weight basis, analyzed by HRGC/HRMS Organochlorine Pesticide Results Concentrations in ng/g (ppb) wet A. MethodsiSamples were collected by the Delaware Department of Natural Resources and Environmental Control (DNREC).TMetals were analyzed by the DNREC's Environmental Services Section (ESS) Laboratory.iOrganic contaminants were analyzed by the Midwest Research Institute (MRI) under contract with the DNREC.Field procedures for sample collection followed DNREC ESS Standard Operating Procedure No. 500 ("Field Procedures for Fish Sample Handling").Procedures for dissection, tissue grinding, and sample storage followed DNREC ESS Standard Operating Procedure No. 501 ("Processing of Finfish for Chemical Analyis"). WLaboratory methods for metals are described in DNREC ESS Standard Operating Procedures.CLaboratory methods for organic contaminants are fully described in:`Institute for the Delaware Department of Natural Resources and Environmental Control, Dover, DE.)Briefly with regard to chemical analyses,Metals other than mercury and zinc were analyzed using Graphite Furnace Atomic Absorption (GFAA). Zinc was analyzed using Inductively Coupled Argon Plasma (ICAP).LMercury was analyzed using Cold Vapor Atomic Absorption Spectrometry (CVAA).Dioxins, furans, and coplanar PCB congeners were analyzed by High Resolution Gas Chromatography/High Resolution Mass Spectrometry (HRGC/HRMS).}All other organic compounds were analyzed by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS).B. Quality AssuranceQuality assurance testing for metals included matrix spike and matrix spike duplicate analyses. Results of those analyses are on file at the DNREC ESS Laboratory.Quality assurance procedures for organic analyses included method blanks, matrix spikes, matrix spike duplicates, and percent recoveries for internal standardsBand surrogate standards. Results of QA testing are documented in:|Midwest Reseach Institute. 1998. Analysis of Fish Tissue Samples for PCDDs, PCDFs, Congener-Specific PCBs, and Pesticides {from Selected Delaware Stream Basins, FY '98 Final Report (MRI Project No. 4892). Report prepared by the Midwest Research Arsenic Cadmium Copper Lead MercurySeleniumZinc (ppm) 1.11< 0.02 0.39< 0.12 0.178 0.43 4.39 0.73 0.49 0.224 0.56 4.660.13 J0.14 J< 0.20.12 J<0.20.11 J0.005 J0.1 J0.19 J0.07 J0.09 J0.006 J0.08 J<0.02<0.12Notes:East of Big Stone Beach, DECherry Island Flats, DE Yorklyn, DENoxontown Pond, DE% LipidDiPCB(8) TriPCB(18) TriPCB(28) TriPCB(37) TetraPCB(42) TetraPCB(44) TetraPCB(47) TetraPCB(49) TetraPCB(52) TetraPCB(60) TetraPCB(64) TetraPCB(66) TetraPCB(70) TetraPCB(74) TetraPCB(80) PentaPCB(82)PentaPCB(84/101) PentaPCB(86) PentaPCB(87) PentaPCB(91) PentaPCB(92) PentaPCB(95) PentaPCB(97) PentaPCB(99)PentaPCB(105/127) PentaPCB(110) PentaPCB(114) PentaPCB(118) PentaPCB(119) PentaPCB(120) PentaPCB(123)HexaPCB(128/167) HexaPCB(137) HexaPCB(138) HexaPCB(141) HexaPCB(146) HexaPCB(149) HexaPCB(151) HexaPCB(153) HexaPCB(156) HexaPCB(157) HexaPCB(158) HexaPCB(166) HexaPCB(168)HeptaPCB(170/190) HeptaPCB(171) HeptaPCB(174) HeptaPCB(177) HeptaPCB(179) HeptaPCB(180) HeptaPCB(183) HeptaPCB(185) HeptaPCB(187) HeptaPCB(191) HeptaPCB(189) OctaPCB(194) OctaPCB(195)OctaPCB(196/203) OctaPCB(198) OctaPCB(200) OctaPCB(201) OctaPCB(205) NonaPCB(206) NonaPCB(207) NonaPCB(208) DecaPCB(209)Sum of CongenersNote:U(2.5)Y1. U(#)=Compound not detected. Value in parentheses is the instrumental detection limit.i1. U(#)=Compound not detected. Value in parentheses is the detection limit based on the lowest standard.+B. PCB Homolog Data, ng/g wet weight basisMonoDiTriTetraPentaHexaHeptaOctaNonaDecaSum of Homologs U(2.5) (1) U( .123)U( .594) U(.00937) U( .0297) U( .0203)U( .188)U( .196)U( .14) U( .0784)U( .214) U( .0603) U( .0797) U( .0601) U( .0948)U( .168)U( .175)U( .125) U( .0831)U( 2.14)U( 5.19)U( .257)U( 5.05)U( .208)U( .12) U( .0669) U( .0874) U( .0276) Total TCDF Total TCDD U( .0341) U( .0343) U( .0339) U( .0469) U( .0709) U( .0355)U( .157)U( .134)U( .381)U( .286)U( .113)U( .133) U( .0823) U( .0533) U( .0762) U( 6.79E-03)U( .1) U( .0826)U( .197)U( .205) U( .0216) U( 8.74E-03)U( 1.8) U( .0664)U( 4.27) U( 8.49E-03) U( 7.44E-03)U( .216)U( .21)U( 3.89)U( .178) U( .0167)U( .102) U( .0574) U( .0315) U( .0759)U( .016) U( .0221) U( .0258) U( .0115)77-TCB>83081-TCB126-PeCB127-PeCBU( .23)U( .183)U( .164)U( .105)U( .129) U( .0184)U( .229)U( .396)U( .144)U( .177) U( .0557) U( .0658) U( .0816) U( .0832)169-HxCBQB. Non-Ortho Coplanar PCB Raw Data, pg/g wet weight basis, analyzed by HRGC/HRMS U( .79 empc) U( .577 empc) U( .468 empc) U( 1.01 empc) U( .237 empc) U( .117 empc) U( .093 empc) U( .113 empc) U( .083 empc) U( .57 empc) U( .153 empc)U( .0946 empc) U( .112 empc) U( .125 empc) U( .34 empc) U( .273 empc) U( .348 empc)U( .0502 empc) U( .057 empc) U( .111 empc) U( .298 empc) U( .485 empc) U( .42 empc) U( .434 empc) U( .174 empc) U( .269 empc) U( .24 empc) U( .152 empc) U( .196 empc) U( .185 empc) U( .114 empc)U( .0884 empc)U( .0707 empc)U( .0776 empc) U( .126 empc)U( .0658 empc) U( .163 empc) U( .225 empc) U( .156 empc) U( .151 empc) U( .119 empc) U( .105 empc)U( .0537 empc)U( .0667 empc)U( .0772 empc)U( .0731 empc)U( .0657 empc)U( .0829 empc) U( .248 empc)U( .0862 empc) U( .18 empc)U( .0226 empc)U( .0127 empc)U( .0101 empc)U( .0219 empc)U( .0213 empc)U( .0634 empc) U( .211 empc) U( .199 empc) U( .179 empc) U( .699 empc)U( .0464 empc)U( .0757 empc) U( .051 empc)U( .0476 empc)U( .0455 empc) U( .183 empc) U( .213 empc) U( .14 empc) U( .201 empc) U( .668 empc) U( .851 empc) U( .822 empc) U( .305 empc) U( .122 empc) U( .091 empc) U( .107 empc) U( .103 empc)U( .0677 empc)U( .0421 empc)U( .0417 empc) U( 3.98 empc) U( 3.91 empc) U( 2.31 empc) U( 9.78 empc) U( 3.14 empc) U( 34 empc) U( 7.59 empc) U( .142 empc) U( .108 empc) U( .073 empc)U( .0841 empc) U( .266 empc)U( .0664 empc)U( .0625 empc)U( .0236 empc)U( .0451 empc) U( .319 empc) U( .209 empc) U( .158 empc) U( .313 empc) U( .198 empc) U( .386 empc) U( .293 empc) U( .187 empc) U( .169 empc) U( .189 empc) U( .127 empc) U( 1.53 empc) U( .962 empc)U( 2.69 empc&)U( 4.95 empc&)U( 4.51 empc&)U( 3.45 empc&) U( 1.1 empc&)U( 1.94 empc&)<h U( 1.42 empc&)U( 1.29 empc&)U( .805 empc&)U( .827 empc&)U( .188 empc&)U( .444 empc&)U( .0558 empc&)U( 1.01 empc&)U( .797 empc&)U( 2.93 empc&)U( .674 empc&)U( 14.8 empc&)U( 10.1 empc&)U( 17.8 empc&)U( 2.64 empc&)U( 5.54 empc&)U( .503 empc&)U( 2.23 empc&)U( .692 empc&) U( 1.5 empc&)U( .499 empc&)U( .405 empc&) U( .58 empc&) U( .71 empc&)U( .107 empc&)U(.0956 empc&)U( 35.2 empc&)U( 23.8 empc&)U( 11.2 empc&)U( 1.69 empc&)U( 5.22 empc&)U( 1.25 empc&)U( 3.82 empc&)U( 1.52 empc&)U( 1.03 empc&)U( 1.38 empc&)U( 2.13 empc&)U( .243 empc&)U( .204 empc&)U( .146 empc&)Y2. U(#)=Compound not detected. Value in parentheses is the instrumental detection limit.3. U(# empc)=Compound not detected. Value in parentheses is an estimated maximum possible concentration (empc) detection limit. 4. U(# empc&)=Compound not detected. Value in parentheses is an estimated maximum possible concentration (empc) detection limit based on a possible diphenyl ether interference.2,3,7,8-TCDF (1) 2,3,7,8-TCDD1,2,3,7,8-PeCDF2,3,4,7,8-PeCDF1,2,3,7,8-PeCDD1,2,3,4,7,8-HxCDF1,2,3,6,7,8-HxCDF2,3,4,6,7,8-HxCDF1,2,3,7,8,9-HxCDF1,2,3,4,7,8-HxCDD1,2,3,6,7,8-HxCDD1,2,3,7,8,9-HxCDD1,2,3,4,6,7,8-HpCDF1,2,3,4,7,8,9-HpCDF1,2,3,4,6,7,8-HpCDDOCDFOCDD Total PECDF Total PECDD Total HXCDF Total HXCDD Total HPCDF Total HPCDD U( .0853) (2) U( .744 empc) (3) U( 1.28 empc&) (4) U( 1.23 empc) U( 1.2 empc) U( 1.73 empc) U( .681 empc)2. U(# empc)=Compound not detected. Value in parentheses is an estimated maximum possible concentration (empc) detection limit. U( .0204) (1) U( .623 empc) (2) Sum of DDD,DDE,DDTcis Chlordane trans Chlordane cis Nonachlortrans Nonachlor OxychlordaneSum of ChlordanesDicofolDieldrin Endosulfan I Endosulfan IIEndrinHeptachlor EpoxideHexachlorobenzeneLindaneMirexU(10) U(10) (1) Sample DescriptionOFY '98 Toxics in Biota Monitoring Data for the Delaware Estuary and Tributariesa1. TCDF should be considered a maximium because the DB-5 column is not specific for this isomer. J = Analyte present. Reported value is estimated. 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