ࡱ> /. I@\p Rick Greene Ba==x<X/#8X@"1Arial1Arial1Arial1Arial1Arial1Arial1Arial1Arial1Arial"$"#,##0_);\("$"#,##0\)!"$"#,##0_);[Red]\("$"#,##0\)""$"#,##0.00_);\("$"#,##0.00\)'""$"#,##0.00_);[Red]\("$"#,##0.00\)7*2_("$"* #,##0_);_("$"* \(#,##0\);_("$"* "-"_);_(@_).))_(* #,##0_);_(* \(#,##0\);_(* "-"_);_(@_)?,:_("$"* #,##0.00_);_("$"* \(#,##0.00\);_("$"* "-"??_);_(@_)6+1_(* #,##0.00_);_(* \(#,##0.00\);_(* "-"??_);_(@_) mm/dd/yy0.0                + ) , *       H " !  !  !X    H    !   h !   ! " " `Sample Description Dioxins & Furans3Methods and QA`izBDelaware Department of Natural Resources and Environmental ControlRData and information in this spreadsheet were obtained from the following sources: 2. DNREC Laboratory Data Files.Sample DescriptionMeanMinimumMaximumDatePortion No.of FishLengthWeight Sample ID WaterbodyLocationLatitude LongitudeSampledSpeciesAnalyzed in Sample(cm)(gm)1. Triangle Laboratories. 1991. Analysis of Samples for the Presence of Polychlorinated Dibenzo-p-Dioxins and Dibenzofurans prepared by Triangle Laboratories, Inc. for the Delaware Department of Natural Resources and Environmental Control, Dover, DE.!Concentrations in pg/g (pptr) wet% Lipid 2,3,7,8-TCDD1,2,3,7,8-PeCDF2,3,4,7,8-PeCDF1,2,3,7,8-PeCDD1,2,3,4,7,8-HxCDF1,2,3,6,7,8-HxCDF2,3,4,6,7,8-HxCDF1,2,3,7,8,9-HxCDF1,2,3,4,7,8-HxCDD1,2,3,6,7,8-HxCDD1,2,3,7,8,9-HxCDD1,2,3,4,6,7,8-HpCDF1,2,3,4,7,8,9-HpCDF1,2,3,4,6,7,8-HpCDDOCDFOCDD Total TCDF Total TCDD Total PECDF Total PECDD Total HXCDF Total HXCDD Total HPCDF Total HPCDDNotes: A. MethodsiSamples were collected by the Delaware Department of Natural Resources and Environmental Control (DNREC).Field procedures for sample collection followed DNREC ESS Standard Operating Procedure No. 500 ("Field Procedures for Fish Sample Handling").Procedures for dissection, tissue grinding, and sample storage followed DNREC ESS Standard Operating Procedure No. 501 ("Processing of Finfish for Chemical Analyis"). B. Quality AssuranceBand surrogate standards. Results of QA testing are documented in:^Dioxins and furans were analyzed by Triangle Laboratories, Inc. under contract with the DNREC.{Triangle Laboratories. 1991. Analysis of Samples for the Presence of Polychlorinated Dibenzo-p-Dioxins and Dibenzofurans ~prepared by Triangle Laboratories, Inc. for the Delaware Department of Natural Resources and Environmental Control, Dover, DE. 9101303 (1)Red Clay CreekYorklyn Brown TroutFillet623.7na150.3 9101588 (2)23.8141.3 9101842 (2)26.0197.0 9101843 (2)24.5170.41. The fish in this sample did not come from the Red Clay Creek. They were hatchery fish that served as controls in a recapture study of stocked trout in the Red Clay Creek. l2. The fish in this sample were recaptured from the Red Clay Creek after being stocked earlier in the year.ALaboratory methods for dioxins and furans are fully described in:Quality assurance procedures included method blanks, matrix spikes, matrix spike duplicates, and percent recoveries for internal standards 2,3,7,8-TCDFFlagND(0.1)ND(0.2) EMPC(0.43) EMPC(0.51) EMPC(0.12) EMPC(0.18) EMPC(0.37) EMPC(0.38) EMPC(0.80)BND(0.3) EMPC(0.17)ND(0.4) EMPC(0.29) EMPC(0.05)ND(0.9) EMPC(0.56) EMPC(1.1) EMPC(0.34)ND(0.5) EMPC(0.27) EMPC(0.28) EMPC(0.19)ND(1.0) EMPC(0.33)EMPC(0.11) (1)  ND(0.1) (2)B (3)D2. ND(#) = not detected with detection limit listed in parentheses.W1. EMPC(#) = estimated maximum possible concentration with EMPC listed in parentheses.f3. B = analyte found in the associated laboratory method blank sample as well as in the field sample.ODioxin and Furan Uptake Study for Stocked Trout in the Red Clay Creek, Delaware by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (TLI Project No. 18249). Laboratory data report yby High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (TLI Project No. 18249). Laboratory data report Dioxin and Furan Results 39 48 22.5 75 40 50.1 @ W  - " 9   ?VCZ  - w  m I@ [  dMbP?_*+%"??U} } $} $ } m } m ;;       t   u                                               != "> "? x y~ #@H@ "@ "A $B  %C  %D  %D  %E  %D %D !F "> "? x y~ #J@ "@ "A $B  %G  %D  %D  %H  %D %D !I "> "? x y~ #`M@ "@ "A $B  %J  %D  %D  %K  %D %D !L "> "? x y~ #`M@ "@ "A $B  %M  %D  %D  %N  %D %D "32"""""!""$$""$""""""""" "O2"""""!""$$""$""""""""" "P2"""""!""$$""$"""""""""2&   T~DD>@7 I@ ,%03  dMbP?_*+%MHP LaserJet 8000 Series PSw o`XXs_/, $aCustom page 1CDCustom page 2CDCustom page 3CD"`XX??U} } $} } $} } $} } $} m,                               w   ~ $+$~ $R+$~ $J+$~ $N+  $>$ $>$ $>$ $>  $?$ $?$ $?$ $?  $@$ $@$ $@$ $@ ~ %p|@ %T~ %v@ %T~ %v@ %T~ %0y@ T  $n~ 2@ $` $V  $o V $` $g # $V _ $a $h $ $V V~ 5@ $i % $V _ $_ $a ( $W p~ G@ ^~ @T@ ^~ %? ^ *~ )@ ^~ @p@ ^~ y@ ^~ %`}@ ^ S $X ^~ ^@ ^~ @ ^~  r@ ^  $U U U V  $U~ (@ b j  $U V V _  $U U c V ! $Y ^ V V k ^ " $U V V _ & $U V~ 0@ _ ' $V _ _ a )~ a@ ^ X ^ d l , $Z~ 2@ e V . $[ \ f g 0 $\ _~ ? m> 0dddd~FFFFF~~~FFFFbFFFbFF !"#$%()*+ 2 $]~ G@~ @T@~ %?!!! "+ "$X~ "f@~ "`s@~ "`x@ #- #$U~ #(@~ #$@ #j $/ $$Y $V~ $5@ $[ %1 %$U %V~ %4@ %_ (3 )r *q +s|FFFFF>@7 I@ #8);  dMbP?_*+%MHP LaserJet 8000 Series PSw odXXMǣs_/, $dCustom page 1CDCustom page 2CDCustom page 3CD"dXX??U      4 5 : 6 7 Q ; v <   8 R 9 ; v <2      >@7  Oh+'0HPdx  Rick Greene Rick GreeneMicrosoft Excel@^@Rr6@G ՜.+,0 PXh px DNREC  Sample DescriptionDioxins & FuransMethods and QA  Worksheets  !"#$%'()*+,-Root Entry FWorkbook;SummaryInformation(DocumentSummaryInformation8&